Nowadays finding the Easy and Economical way to treat the industrial wastewater is the raising ideas in newer technology. In this work adsorption of methylene blue using various adsorbent such as groundnut shell, and tea waste were used in batch studies at a constant dye concentration of 300 mg/l, adsorbent dose of 0.5 gm groundnut shell powder, and Spent tea powder. The time of Agitation was varied by 20, 40, 60, 80, 100 min. After the time of agitation of 100 min, Maximum dye removal of 86% was observed in spent tea powder and 80% was observed in Groundnut shell powder.